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Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi

Year 2015, Volume: 5 Issue: 1, 36 - 42, 10.07.2015

Niyaz Berk Esra Barım , Cumhur Kırılmış

Abstract

Bu çalışmada; 2-asetil-benzofuran bromlanarak bromoasetilbenzofuran elde edildi. Primer ve
sekonder aminlerin ditiyokarbamat tuzları ile α-haloketonun reaksiyonu sonucunda oluşan
ürünler incelendi. Elde edilen ditiyokarbamat esterlerinin yapıları 1H-NMR, 13C-NMR ve FTIR
gibi spektroskopik yöntemler kullanılarak karakterize edildi.

Keywords

Benzofuran α-Haloketon Ditiyokarbamat Tuzu Ditiyokarbamat esterleri

References

  • T. L. Gilchrist, Heterocyclic Chemistry, Longman Group UK Lim. England, 1985, 174.
  • D. Bogdal, M. Warzala, Tetrahedron, 2000, 56, 8769-8773.
  • M. W. Khan, M. J. Alam, M. A. Rashid, R. Chowdhury, Bioorganic & Medicinal Chemistry, 2005, 13, 4796-4805.
  • C. Kırılmış, M. Ahmedzade, S. Servi, M. Koca, A. Kizirgil, C. Kazaz, European Journal of Medicinal Chemistry, 2008, 43, 300-308.
  • C. L. Kao, J. W. Chern, J. Org. Chem., 2002, 67, 6772-6787.
  • K. E. Kinnamon, B. T. Poon, W. L. Hanson, V.B. Waits, Experimental Parasitology, 1998, 89, 251-256.
  • M. Kulka, Canadian Journal of Chemistry, 1956, 34, 1093-1100.
  • L. Drobnica, P. Kristian, J. Augustin, Chichester: John Wiley and Sons., 1977.
  • K. Hirai, H. Sugimoto, T. Ishiba,. Reaction of 1,3-Dithiolium Cation with Xanthate and Dithiocarbamate Anions, Journal of Organic Chemistry, 1977, 42 (9), 1543-1549.

Synthesis of Benzofuran Derivatives Dithiocarbamate Esthers

Year 2015, Volume: 5 Issue: 1, 36 - 42, 10.07.2015

Niyaz Berk Esra Barım , Cumhur Kırılmış

Abstract

In this study; bromoacetylbenzofuran was obtained by bromizing 2-acetyl-benzofuran. Dithiocarbamatesalts of primary and secondary amines with products of α-haloketon reaction were examined. The structures of derived dithiocarbamate esters were characterized by 1HNMR, 13C-NMR and FT-IR spectroscopic methods.

Keywords

Benzofuran α-haloketone Dithiocarbamate Salt Dithiocarbamate Esthers

References

  • T. L. Gilchrist, Heterocyclic Chemistry, Longman Group UK Lim. England, 1985, 174.
  • D. Bogdal, M. Warzala, Tetrahedron, 2000, 56, 8769-8773.
  • M. W. Khan, M. J. Alam, M. A. Rashid, R. Chowdhury, Bioorganic & Medicinal Chemistry, 2005, 13, 4796-4805.
  • C. Kırılmış, M. Ahmedzade, S. Servi, M. Koca, A. Kizirgil, C. Kazaz, European Journal of Medicinal Chemistry, 2008, 43, 300-308.
  • C. L. Kao, J. W. Chern, J. Org. Chem., 2002, 67, 6772-6787.
  • K. E. Kinnamon, B. T. Poon, W. L. Hanson, V.B. Waits, Experimental Parasitology, 1998, 89, 251-256.
  • M. Kulka, Canadian Journal of Chemistry, 1956, 34, 1093-1100.
  • L. Drobnica, P. Kristian, J. Augustin, Chichester: John Wiley and Sons., 1977.
  • K. Hirai, H. Sugimoto, T. Ishiba,. Reaction of 1,3-Dithiolium Cation with Xanthate and Dithiocarbamate Anions, Journal of Organic Chemistry, 1977, 42 (9), 1543-1549.
There are 9 citations in total.

Details

Primary Language Turkish
Subjects Engineering
Journal Section Chemistry
Authors

Niyaz Berk This is me

Esra Barım

Cumhur Kırılmış

Publication Date July 10, 2015
Submission Date July 10, 2015
Published in Issue Year 2015 Volume: 5 Issue: 1

Cite

APA Berk, N., Barım, E., & Kırılmış, C. (2015). Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi. Adıyaman University Journal of Science, 5(1), 36-42.
AMA Berk N, Barım E, Kırılmış C. Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi. ADYU J SCI. June 2015;5(1):36-42.
Chicago Berk, Niyaz, Esra Barım, and Cumhur Kırılmış. “Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi”. Adıyaman University Journal of Science 5, no. 1 (June 2015): 36-42.
EndNote Berk N, Barım E, Kırılmış C (June 1, 2015) Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi. Adıyaman University Journal of Science 5 1 36–42.
IEEE N. Berk, E. Barım, and C. Kırılmış, “Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi”, ADYU J SCI, vol. 5, no. 1, pp. 36–42, 2015.
ISNAD Berk, Niyaz et al. “Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi”. Adıyaman University Journal of Science 5/1 (June 2015), 36-42.
JAMA Berk N, Barım E, Kırılmış C. Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi. ADYU J SCI. 2015;5:36–42.
MLA Berk, Niyaz et al. “Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi”. Adıyaman University Journal of Science, vol. 5, no. 1, 2015, pp. 36-42.
Vancouver Berk N, Barım E, Kırılmış C. Benzofuran Türevli Ditiyokarbamat Esterlerinin Sentezi. ADYU J SCI. 2015;5(1):36-42.
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