Research Article
Seramik Karoların Altın Dekorasyonunda Katodik Ark-FBB TiN Kaplama Proses Parametrelerinin Optimizasyonu
Abstract
Bu
çalışmada, seramik karo yüzeyinde dekoratif altın renginde TiN kaplamalar
üretmek için Katodik Ark FBB proses parametrelerinin optimizasyonu
amaçlanmıştır. Kaplama ünitesinde; altlık malzemesi olarak sırlı seramik
karolar, katot olarak saf Ti diskler ve reaktif gaz olarak da nitrojen (N2)
kullanılmıştır. Kaplama işlemi; sabit
biriktirme süresinde (90 sn), katod akımı (100-150-200A) ve N2 akış
oranı (550-650-750 sccm) değiştirilerek gerçekleştirilmiştir. Üretilen
kaplamaların L*a*b* renk
parametreleri spektrafotometre ile ölçülmüş ve ticari TiN kaplamaların L*a*b* değerleri ile
karşılaştırılmıştır. Sonuç olarak, TiN stokiyometrisine yakın olduğu düşünülen
proses parametreleri ile (550 sccm-150 A ve 650 sccm-200 A) ticari TiN
kaplamalara benzer altın renginde kaplamalar üretilmiştir.
References
- Alberdi, A.A., Lucas M.F., Belda P.A. and Bueno, Z.R.M., 2005. Method of producing ceramic tiles having a metallic finish and the tile thus produced. Europ. Patent No: EP 1498402 A1
- Alves, L.A., Sagas, J.C., Damiao, A.J. and Fontana, L.C., 2015. Drude’s model optical parameters and the color of TiNx films obtained through reflectivity measurements. Braz. J. Physics, 45, 59-63.
- Kim, H.J. and Joun, M.S., 2007. Effects of deposition temperature and time on the surface characteristics of TiN-coated high-speed steel by arc ion plating. Journal of Mechanichal Science and Technology, 21, 575-584.
- Larpkiattaworn, S., Chokwatvikul, C., Surinphong, S. and Termsuksaward, P., 2013. Properties of (Ti,Al)N film prepared by PVD cathodic arc. Suranaree J. of Science and Technology, 20 (3), 221-226.
- Lousa, A., Esteve, J., Mejia, J.P. and Devia, A., 2007. Influence of deposition pressure on the structural mechanical and decorative properties of TiN thin films deposited by cathodic arc evaporation, Vacuum, 81, 1507-1510.
- Manova, D., Gerlach, J.W. and Mandl, S., 2010. Thin film deposition using energetic ions. Materials, 2, 4109-4141.
- Mubarak, A., Hamzah, E. and Toff, M.R.M., 2005. Review of PVD techniques for hard coating, Jurnal Mekanikal, 20, 42-51.
- Niyomsoan, S., Grant, W., Olson, D.L and Mishra, B., 2002. Variation of color in titanium and zirconium nitride decorative thin films. Thin Solid Films, 415,187-194.
- Öncel, S., 2002. Katodik ark FBB yöntemi ile dekoratif amaçlı Cr-O-N kaplamaların üretilmesi, Yüksek Lisans Tezi, İTÜ Fen Bilimleri Enstitüsü, İstanbul, 68.
- Richert M., Mazurkiewicz, A. and Smolik, J., 2010. Chromium carbide coatings obtained by the hybrid PVD methods. Journal of Achievements in Materials and Manufacturing Engineering, 43, 145-152.
- Sönmezoğlu, S., Koç, M. ve Akın, S., 2012. İnce film üretim teknikleri. Erciyes Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 28(5), 389-401.
- Vaz, F., Machado, P., Rebouta, L. and Mendes, J.A., 2002. Physical and morphological characterization of reactively magrettron sputtered TiN films. Thin Solid Films, 421-428.
- Zeghni, A., 2003. The effect of thin film coatings and nitriding on the mechanical properties and wear resistance of tool steel, Master Thesis, School of Mechanical and Manufacturing Engineering, Dublin City University, Dublin, 150.
Year 2019,
Volume: 19 Issue: 1, 186 - 192, 28.05.2019
Abstract
References
- Alberdi, A.A., Lucas M.F., Belda P.A. and Bueno, Z.R.M., 2005. Method of producing ceramic tiles having a metallic finish and the tile thus produced. Europ. Patent No: EP 1498402 A1
- Alves, L.A., Sagas, J.C., Damiao, A.J. and Fontana, L.C., 2015. Drude’s model optical parameters and the color of TiNx films obtained through reflectivity measurements. Braz. J. Physics, 45, 59-63.
- Kim, H.J. and Joun, M.S., 2007. Effects of deposition temperature and time on the surface characteristics of TiN-coated high-speed steel by arc ion plating. Journal of Mechanichal Science and Technology, 21, 575-584.
- Larpkiattaworn, S., Chokwatvikul, C., Surinphong, S. and Termsuksaward, P., 2013. Properties of (Ti,Al)N film prepared by PVD cathodic arc. Suranaree J. of Science and Technology, 20 (3), 221-226.
- Lousa, A., Esteve, J., Mejia, J.P. and Devia, A., 2007. Influence of deposition pressure on the structural mechanical and decorative properties of TiN thin films deposited by cathodic arc evaporation, Vacuum, 81, 1507-1510.
- Manova, D., Gerlach, J.W. and Mandl, S., 2010. Thin film deposition using energetic ions. Materials, 2, 4109-4141.
- Mubarak, A., Hamzah, E. and Toff, M.R.M., 2005. Review of PVD techniques for hard coating, Jurnal Mekanikal, 20, 42-51.
- Niyomsoan, S., Grant, W., Olson, D.L and Mishra, B., 2002. Variation of color in titanium and zirconium nitride decorative thin films. Thin Solid Films, 415,187-194.
- Öncel, S., 2002. Katodik ark FBB yöntemi ile dekoratif amaçlı Cr-O-N kaplamaların üretilmesi, Yüksek Lisans Tezi, İTÜ Fen Bilimleri Enstitüsü, İstanbul, 68.
- Richert M., Mazurkiewicz, A. and Smolik, J., 2010. Chromium carbide coatings obtained by the hybrid PVD methods. Journal of Achievements in Materials and Manufacturing Engineering, 43, 145-152.
- Sönmezoğlu, S., Koç, M. ve Akın, S., 2012. İnce film üretim teknikleri. Erciyes Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 28(5), 389-401.
- Vaz, F., Machado, P., Rebouta, L. and Mendes, J.A., 2002. Physical and morphological characterization of reactively magrettron sputtered TiN films. Thin Solid Films, 421-428.
- Zeghni, A., 2003. The effect of thin film coatings and nitriding on the mechanical properties and wear resistance of tool steel, Master Thesis, School of Mechanical and Manufacturing Engineering, Dublin City University, Dublin, 150.
There are 13 citations in total.
Details
| Primary Language | Turkish |
|---|---|
| Subjects | Engineering |
| Journal Section | Articles |
| Authors | |
| Publication Date | May 28, 2019 |
| Submission Date | April 19, 2018 |
| Published in Issue | Year 2019 Volume: 19 Issue: 1 |