FARKLI HASAT ZAMANLARININ BERGAMOT (Citrus bergamia Risso et Poiteau) KABUK UÇUCU YAĞININ BAZI KALİTE PARAMETRELERİNE ETKİSİ
Year 2020,
Volume: 49 Issue: 2, 67 - 73, 03.12.2020
Muharrem Gölükçü
,
Haluk Tokgöz
,
Demet Yıldız Turgut
Abstract
Turunçgiller dünyadan tarımı en çok yapılan meyve türlerindendir. Bunlardan biriside bergamot olup, bergamot daha çok uçucu yağ üretiminde kullanılmaktadır. Diğer turunçgil türlerinde olduğu gibi bergamot uçucu yağının bileşimi de hasat zamanı, yetiştirilme şartları, üretim metodu gibi faktörlere göre değişebilmektedir. Bu çalışmada farklı hasat zamanlarının bergamot kabuklarının uçucu yağ verimi ve uçucu yağ bileşimi üzerine etkisi araştırılmıştır. Örneklerin uçucu yağ içeriği klevenger düzeneğinde hidrodistilasyon yöntemi ile uçucu yağ bileşimi ise GC-MS/FID cihazı ile belirlenmiştir. Bergamot kabuk uçucu yağ miktar ve bileşiminde hasat zamanına göre değişimler olduğu tespit edilmiştir. Örneklerin uçucu yağ miktarı %2.11-2.99 aralığında değişim göstermiştir. Araştırma kapsamında analiz edilen uçucu yağ örneklerinde 14 farklı bileşenin bulunduğu tespit edilmiştir. Örneklerin bileşiminde makro düzeyde limonen, linalool ve linalil asetat bulunmakta olup oranları hasat zamanına göre sırasıyla %46.20-46.98, %13.42-20.22, %12.20-15.91 aralığında dağılım göstermiştir. Araştırma bulguları bergamot için hasat zamanın uçucu yağ verim ve bileşimi açısından önemli etkiye sahip olduğunu göstermiştir.
References
- Anonim, 2009. TS ISO 280, Eteri yağlar-kırılma indisi tayini. Türk Standartları Enstitüsü, Ankara, 8s.
- Anonim, 2011. TS EN ISO 6571, Baharatlar, çeşniler ve tıbbi bitkiler-uçucu yağ muhtevasının tayini (hidrodistilasyon yöntemi). Türk Standartları Enstitüsü, Ankara, 12s.
- Anonim, 2012. TS ISO 592, Eteri yağlar-optik çevirme açısı tayini-polarimetrik metot. Türk Standartları Enstitüsü, Ankara, 8s.
- Babushok, V.I., P.J. Linstrom and I.G. Zenkevich, 2011. Retention indices for frequently reported compounds of plant essential oils. Journal of Physical and Chemical Reference Data, 40(4):1-47.
- Baser, K.H.C., T. Özek and M. Tutas, 1995. Composition of cold pressed bergamot oil from Turkey. Journal of Essential Oil Research, 7(3):341-342.
- Bisignano, G., F. Cimino and A. Saija, 2011. Biological activities of citrus essential oils. pp:529-547. In: Dugo, G., Mondello, L. (Eds), Citrus oils composition, advanced analytical techniques, contaminants, and biological activity. CRC Press, Taylor & Francis Group, London, UK. 548p.
- Costa, R., P. Dugo, M. Navarra, V. Raymo, G. Dugo, and L. Mondello, 2010. Study on the chemical composition variability of some processed bergamot (Citrus bergamia) essential oils. Flavour and Fragrance Journal, 25:4-12.
- Dugo, G. and I. Bonaccorsi, 2014. Citrus bergamia bergamot and its derivatives. Taylor & Francis Group, LLC CRC Press, 549p.
- Dugo, G., A. Controneo, I. Bonaccorsi and A. Trozzi, 2011. Composition of the volatile fraction of citrus peel oils. pp:1-161. In: Dugo, G., Mondello, L. (Eds.), Citrus oils composition, advanced analytical techniques, contaminants, and biological activity. CRC Press, Taylor & Francis Group. London, UK. 548p.
- Dugo, G., A. Cotroneo, A. Verzera, M.G. Donato and R. Del Duce, 1991. Genuineness characters of Calabrian bergamot essential oil. Flavour and Fragrance Journal, 6:39-56.
- Dugo, G. and A. Di Giacomo, 2002. Citrus the genus citrus. Taylor & Francis Group, London, UK. 642p.
- Düzgüneş, O., T. Kesici, O. Kavuncu ve F. Gürbüz, 1987. Araştırma ve deneme metotları. Ankara Üniversitesi, Ziraat Fakültesi Yayın No: 1021, Ankara, 229s.
- Espina, L., M. Somolinos, S. Loran, P. Conchello, D. Garcia and R. Pagan, 2011. Chemical composition of commercial citrus fruit essential oils and evaluation of their antimicrobial activity acting alone or in combined processes. Food Control, 22: 896-902.
- Figoli, A., L. Donato, R. Carnevale, R. Tundis, G.A. Statti, F. Menichini and E. Drioli, 2006. Bergamot essential oil extraction by pervaporation. Desalination, 193:160-165.
- Fisher, K. and C.A. Phillips, 2006. The effect of lemon, orange and bergamot essential oils and their components on the survival of campylobacter jejuni, escherichia coli O157, Listeria monocytogenes, bacillus cereus and staphylococcus aureus in vitro and in food systems. Journal of Applied Microbiology, 101:1232-1240.
- Franz, C. and J. Novak, 2010. Sources of essential oils. pp:39-82. In: Başer, K.H.C., Buchbauer, G. (Eds.), Handbook of essential oils science, technology and applications. CRC Press, USA, 975p.
- Furneri, P.M., L. Mondello, G. Mandalari, D. Paolino, P. Dugo, A. Garozzo and G. Bisignano, 2012. In vitro antimycoplasmal activity of Citrus bergamia essential oil and its major components. European Journal of Medicinal Chemistry, 52:66-69.
- Gölükcü, M., R. Toker, H. Tokgöz ve D. Yıldız Turgut, 2015. Farklı yöntemlerle elde edilen turunç (Citrus aurantium L.) kabuk yağlarının uçucu yağ bileşimleri. Derim, 32(2):161-170.
- Kırbaşlar, F.G., A. Tavman, B. Dülger and G. Türker, 2009. Antimicrobial activity of Turkish citrus peel oils. Pakistan Journal of Botany, 41(6):3207-3212.
- Kimball, D.A., 1999. Citrus processing a complete guide. A Chapman & Hall Food Science Book, Aspen Publishers, Inc. Gaithersburg, Maryland, USA, 450p.
- Kirbaslar, F.G., S.I. Kirbaslar and U. Dramur, 2001. The compositions of Turkish bergamot oils produced by cold-pressing and steam distillation. Journal of Essential Oil Research, 13(6):411-415.
- Ladaniya, M.S., 2008. Citrus fruit biology, technology and evaluation. Academic Press, San Diego, USA. 575p.
- Nabiha, B., E.O. Abdelfatteh, K. Faten, C. Herve and C.M. Moncef, 2010. Chemical composition of bergamot (Citrus bergamia Risso) essential oil obtained by hydrodistillation. Journal of Chemistry and Chemical Engineering, 4(4):60-62.
- Navarra, M., C. Mannucci, M. Delbo and G. Calapai, 2015. Citrus bergamia essential oil: from basic research to clinical application. Frontiers in Pharmacology, 6:1-7.
- Özdemir, K.S., N. Azarabadi and A. Topuz, 2018. Microencapsulation of bergamot peel essential oil with gum Arabic and maltodextrin blends: stability and release characteristics of the essential oil compounds. Gıda, 43(6):957-970.
- Poiana, M., R. Fresa and B. Mincione, 1999. Supercritical carbon dioxide extraction of bergamot peels. Extraction kinetics of oil and its components. Flavour and Fragrance Journal, 14:358-366.
- Sawamura, M., Y. Onishi, J. Ikemoto, N.T.M. Tu and N.T.L. Phi, 2006. Characteristic odour components of bergamot (Citrus bergamia Risso) essential oil. Flavour and Fragrance Journal, 21:609-615.
- Tisserand, R. and R. Young, 2014. Essential oil safety. Churchill Livingstone Elsevier, London UK, 779p.
- Verzera, A., A. Trozzi, F. Gazea, G. Cicciarello and A. Cotroneo, 2003. Effects of rootstock on the composition of bergamot (Citrus bergamia Risso et Poiteau) essential oil. Journal of Agricultural and Food Chemistry, 51:206-210.
- Yıldız Turgut, D., M. Gölükcü, R. Toker ve H. Tokgöz, 2014. Bergamot (Citrus bergamia) esansının uçucu yağ bileşimi. 2. Tıbbi ve Aromatik Bitkiler Sempozyumu, 23-25.09.2014. Yalova, 65s.
HARVEST TIMES EFFECT ON SOME QUALITY PARAMETERS OF BERGAMOT (Citrus bergamia Risso et Poiteau) PEEL ESSENTIAL OIL
Year 2020,
Volume: 49 Issue: 2, 67 - 73, 03.12.2020
Muharrem Gölükçü
,
Haluk Tokgöz
,
Demet Yıldız Turgut
Abstract
Citrus fruits are one of the most common fruit species in the world. Bergamot is one of the important species and used extensively in essential oil production. As in other citrus species, the composition of bergamot essential oil may vary depending on many factors such as harvest time, growing conditions, production method etc. In this study, the effect of harvest times on the essential oil content and the composition of bergamot peel were investigated. The essential oil content of the samples was determined by hydrodistillation method in the Clevenger apparatus and the essential oil composition was determined by chromatographic method with GC-MS/FID apparatus. Bergamot peel essential oil content and composition were varied according to the harvest times. Essential oil content of the samples was ranged from 2.11% to 2.99% with respect to harvesting times. Totally, 14 components were determined in these essential oil samples. Limonene, linalool and lineally acetate were main components and their ratios were determined as 46.20-46.98%, 13.42-20.22% and 12.20-15.91% respectively. It is widely used in the production of essential oil. Results showed that harvesting times for bergamot has important effect on essential oil content and composition.
References
- Anonim, 2009. TS ISO 280, Eteri yağlar-kırılma indisi tayini. Türk Standartları Enstitüsü, Ankara, 8s.
- Anonim, 2011. TS EN ISO 6571, Baharatlar, çeşniler ve tıbbi bitkiler-uçucu yağ muhtevasının tayini (hidrodistilasyon yöntemi). Türk Standartları Enstitüsü, Ankara, 12s.
- Anonim, 2012. TS ISO 592, Eteri yağlar-optik çevirme açısı tayini-polarimetrik metot. Türk Standartları Enstitüsü, Ankara, 8s.
- Babushok, V.I., P.J. Linstrom and I.G. Zenkevich, 2011. Retention indices for frequently reported compounds of plant essential oils. Journal of Physical and Chemical Reference Data, 40(4):1-47.
- Baser, K.H.C., T. Özek and M. Tutas, 1995. Composition of cold pressed bergamot oil from Turkey. Journal of Essential Oil Research, 7(3):341-342.
- Bisignano, G., F. Cimino and A. Saija, 2011. Biological activities of citrus essential oils. pp:529-547. In: Dugo, G., Mondello, L. (Eds), Citrus oils composition, advanced analytical techniques, contaminants, and biological activity. CRC Press, Taylor & Francis Group, London, UK. 548p.
- Costa, R., P. Dugo, M. Navarra, V. Raymo, G. Dugo, and L. Mondello, 2010. Study on the chemical composition variability of some processed bergamot (Citrus bergamia) essential oils. Flavour and Fragrance Journal, 25:4-12.
- Dugo, G. and I. Bonaccorsi, 2014. Citrus bergamia bergamot and its derivatives. Taylor & Francis Group, LLC CRC Press, 549p.
- Dugo, G., A. Controneo, I. Bonaccorsi and A. Trozzi, 2011. Composition of the volatile fraction of citrus peel oils. pp:1-161. In: Dugo, G., Mondello, L. (Eds.), Citrus oils composition, advanced analytical techniques, contaminants, and biological activity. CRC Press, Taylor & Francis Group. London, UK. 548p.
- Dugo, G., A. Cotroneo, A. Verzera, M.G. Donato and R. Del Duce, 1991. Genuineness characters of Calabrian bergamot essential oil. Flavour and Fragrance Journal, 6:39-56.
- Dugo, G. and A. Di Giacomo, 2002. Citrus the genus citrus. Taylor & Francis Group, London, UK. 642p.
- Düzgüneş, O., T. Kesici, O. Kavuncu ve F. Gürbüz, 1987. Araştırma ve deneme metotları. Ankara Üniversitesi, Ziraat Fakültesi Yayın No: 1021, Ankara, 229s.
- Espina, L., M. Somolinos, S. Loran, P. Conchello, D. Garcia and R. Pagan, 2011. Chemical composition of commercial citrus fruit essential oils and evaluation of their antimicrobial activity acting alone or in combined processes. Food Control, 22: 896-902.
- Figoli, A., L. Donato, R. Carnevale, R. Tundis, G.A. Statti, F. Menichini and E. Drioli, 2006. Bergamot essential oil extraction by pervaporation. Desalination, 193:160-165.
- Fisher, K. and C.A. Phillips, 2006. The effect of lemon, orange and bergamot essential oils and their components on the survival of campylobacter jejuni, escherichia coli O157, Listeria monocytogenes, bacillus cereus and staphylococcus aureus in vitro and in food systems. Journal of Applied Microbiology, 101:1232-1240.
- Franz, C. and J. Novak, 2010. Sources of essential oils. pp:39-82. In: Başer, K.H.C., Buchbauer, G. (Eds.), Handbook of essential oils science, technology and applications. CRC Press, USA, 975p.
- Furneri, P.M., L. Mondello, G. Mandalari, D. Paolino, P. Dugo, A. Garozzo and G. Bisignano, 2012. In vitro antimycoplasmal activity of Citrus bergamia essential oil and its major components. European Journal of Medicinal Chemistry, 52:66-69.
- Gölükcü, M., R. Toker, H. Tokgöz ve D. Yıldız Turgut, 2015. Farklı yöntemlerle elde edilen turunç (Citrus aurantium L.) kabuk yağlarının uçucu yağ bileşimleri. Derim, 32(2):161-170.
- Kırbaşlar, F.G., A. Tavman, B. Dülger and G. Türker, 2009. Antimicrobial activity of Turkish citrus peel oils. Pakistan Journal of Botany, 41(6):3207-3212.
- Kimball, D.A., 1999. Citrus processing a complete guide. A Chapman & Hall Food Science Book, Aspen Publishers, Inc. Gaithersburg, Maryland, USA, 450p.
- Kirbaslar, F.G., S.I. Kirbaslar and U. Dramur, 2001. The compositions of Turkish bergamot oils produced by cold-pressing and steam distillation. Journal of Essential Oil Research, 13(6):411-415.
- Ladaniya, M.S., 2008. Citrus fruit biology, technology and evaluation. Academic Press, San Diego, USA. 575p.
- Nabiha, B., E.O. Abdelfatteh, K. Faten, C. Herve and C.M. Moncef, 2010. Chemical composition of bergamot (Citrus bergamia Risso) essential oil obtained by hydrodistillation. Journal of Chemistry and Chemical Engineering, 4(4):60-62.
- Navarra, M., C. Mannucci, M. Delbo and G. Calapai, 2015. Citrus bergamia essential oil: from basic research to clinical application. Frontiers in Pharmacology, 6:1-7.
- Özdemir, K.S., N. Azarabadi and A. Topuz, 2018. Microencapsulation of bergamot peel essential oil with gum Arabic and maltodextrin blends: stability and release characteristics of the essential oil compounds. Gıda, 43(6):957-970.
- Poiana, M., R. Fresa and B. Mincione, 1999. Supercritical carbon dioxide extraction of bergamot peels. Extraction kinetics of oil and its components. Flavour and Fragrance Journal, 14:358-366.
- Sawamura, M., Y. Onishi, J. Ikemoto, N.T.M. Tu and N.T.L. Phi, 2006. Characteristic odour components of bergamot (Citrus bergamia Risso) essential oil. Flavour and Fragrance Journal, 21:609-615.
- Tisserand, R. and R. Young, 2014. Essential oil safety. Churchill Livingstone Elsevier, London UK, 779p.
- Verzera, A., A. Trozzi, F. Gazea, G. Cicciarello and A. Cotroneo, 2003. Effects of rootstock on the composition of bergamot (Citrus bergamia Risso et Poiteau) essential oil. Journal of Agricultural and Food Chemistry, 51:206-210.
- Yıldız Turgut, D., M. Gölükcü, R. Toker ve H. Tokgöz, 2014. Bergamot (Citrus bergamia) esansının uçucu yağ bileşimi. 2. Tıbbi ve Aromatik Bitkiler Sempozyumu, 23-25.09.2014. Yalova, 65s.