Research Article
BibTex RIS Cite

Comparison of the Mechanical Properties of Various Microhybrid Dental Composites

Year 2023, Volume: 1 Issue: 3, 58 - 64, 20.12.2023

Abstract

Aim The objective of this study was to investigate the surface microhardness and roughness of several michrohybrid dental composite restorative materials comparatively.
Material and method The study encompassed four distinct brands of microhybrid-type dental composites, including two newly introduced ones, Dentac Myra and Dentac Pergamon, alongside Gradia Direct Posterior and 3M Z250. Additionally, a newly manufactured Parion Flow flowable composite was also included. For surface microhardness testing, 45 composite discs were prepared with a diameter of 5 mm and a thickness of 2 mm for each group (n=9). For surface roughness, 45 composite discs with a diameter of 8 mm and a thickness of 2 mm were prepared (n=9). Surface microhardness was measured using the Vickers Hardness Test device, and surface roughness was measured using a contact profilometer. One-Way ANOVA with Tukey’s HSD analysis and the Kruskal-Wallis H test with Dunnett’s correction were used for intergroup comparisons.
Results Strongly significant differences were observed among groups in terms of microhardness (p < 0.0001; F = 94.75). The highest Vickers hardness number (VHN) was obtained for 3M Z250, while Gradia Direct Posterior exhibited inferior values compared to Myra (p > 0.05) and Pergamon (p = 0.0378). Significant differences were found among groups in terms of surface roughness (p < 0.0001; H = 34.36), with Gradia Direct Posterior having the highest roughness value.
Conclusion Myra and Pergamon demonstrated better performance in terms of surface roughness and microhardness values compared to Gradia Direct Posterior. The similar performance was not observed compared to 3M Z250

Project Number

Yoktur

References

  • Kaizer MR, de Oliveira-Ogliari A, Cenci MS, Opdam NJM, Moraes RR. Do nanofill or submicron composites show improved smoothness and gloss? A systematic review of in vitro studies. Dental Materials. 2014;30(4):e41–78.
  • Nimet Ü, Ülkü SG. Son 10 yılda kompozit rezin restorasyonlar: in vivo ve in vitro çalışmalarla bir derleme. Necmettin Erbakan Üniversitesi Diş Hekimliği Dergisi. 2020;2(3):124–45.
  • Hervás García A, Lozano M, Cabanes Vila J, Barjau Escribano A, Fos Galve P. Composite resins: a review of the materials and clinical indications. 2006;11(2):E215–20.
  • Santerre JP, Shajii L, Leung BW. Relation of dental composite formulations to their degradation and the release of hydrolyzed polymeric-resin-derived products. Critical Reviews in Oral Biology & Medicine. 2001;12(2):136–51.
  • Sideridou ID, Karabela MM. Effect of the amount of 3-methacyloxypropyltrimethoxysilane coupling agent on physical properties of dental resin nanocomposites. Dental Materials. 2009;25(11):1315–24.
  • Hosseinalipour M, Javadpour J, Rezaie H, Dadras T, Hayati AN. Investigation of mechanical properties of experimental Bis‐GMA/TEGDMA dental composite resins containing various mass fractions of silica nanoparticles. Journal of Prosthodontics: Implant, Esthetic and Reconstructive Dentistry. 2010;19(2):112–7.
  • Ritter A V. Sturdevant’s art & science of operative dentistry-e-book. Elsevier Health Sciences; 2017. 470–471 p.
  • Berto-Inga J, Santander-Rengifo F, Ladera-Castañeda M, López-Gurreonero C, Pérez-Vargas AC, Cornejo-Pinto A, et al. Surface Microhardness of Bulk-Fill Resin Composites Handled With Gloves. Int Dent J. 2023;73(4):489–95.
  • Özyurt E. Güncel Rezin Kompozit Materyallerin Fiziksel ve Optik Özelliklerinin Değerlendirilmesi. Selcuk Dental Journal. 2023;10(1):7–11.
  • Bilgili D, Dündar A, Barutçugil Ç, Öcal İB. Farkli cila sistemlerinin kompozit rezinlerin yüzey pürüzlülükleri üzerine etkisi. 7tepe Klinik Dergisi. 2020;16(2):147–53.
  • Sideridou I, Tserki V, Papanastasiou G. Study of water sorption, solubility and modulus of elasticity of light-cured dimethacrylate-based dental resins. Biomaterials. 2003;24(4):655–65.
  • Szalewski L, Wójcik D, Sofińska-Chmiel W, Kuśmierz M, Różyło-Kalinowska I. How the duration and mode of photopolymerization affect the mechanical properties of a dental composite resin. Materials. 2022;16(1):113.
  • Özmen S, Bengü D, ŞenolL AA, Korkut B, Tarçın B, Atalı PY. Tarihi geçmiş kompozit rezinleri kullanmak mümkün mü?: FTIR analizi. Istanbul Kent University Journal of Health Sciences. 2023;2(1):5–11.
  • Cazzaniga G, Ottobelli M, Ionescu A, Garcia-Godoy F, Brambilla E. Surface properties of resin-based composite materials and biofilm formation: A review of the current literature. Am J Dent. 2015;28(6):311–20.
  • Marovic D, Panduric V, Tarle Z, Ristic M, Sariri K, Demoli N, et al. Degree of conversion and microhardness of dental composite resin materials. J Mol Struct. 2013;1044:299–302.
  • Rodrigues-Junior SA, Chemin P, Piaia PP, Ferracane JL. Surface roughness and gloss of actual composites as polished with different polishing systems. Oper Dent. 2015;40(4):418–29.
  • Tofan SA, Todor L, Cosoroabă R, Tănase AD, Todor SA, Popovici RA. Dental Biomaterials in Dental Filling: Why and How to Use? Research and Clinical Medicine Journal. 2021;5(3):11–5.
  • Torres CRG. Modern operative dentistry: Principles for clinical practice. Springer Nature; 2019.
  • Craig RG, Powers JM, Sakaguchi RL. Craig’s restorative dental materials. 13th ed. Mechanical properties. St. Louis: Mosby; 2006. 166–170 p.
  • Caprili S, Mattei F, Mazzatura I, Ferrari F, Gammino M, Mariscotti M, et al. Evaluation of mechanical characteristics of steel bars by non-destructive Vickers micro-hardness tests. Procedia Structural Integrity. 2023;44:886–93.
  • Filija E, Šalinović I. Microhardness testing: can we measure the repair of demineralized lesion? Sonda: List studenata Stomatološkog fakulteta Sveučilišta u Zagrebu. 2022;21(43):44–7.
  • ISO B. 4049: 2019; Dentistry—Polymer-Based Restorative Materials [Internet]. British Standard: London, UK. 2019 [cited 2023 Aug 25]. Available from: https://www.iso.org/standard/67596.html.
  • Çetin AR, Hataysal AE, Aktaş B. Yeni iki tip kompozit materyalin mekanik özelliklerinin karşılaştırılması. Selcuk Dental Journal. 2018;5(3):194–202.
  • Ghavami-Lahiji M, Firouzmanesh M, Bagheri H, Kashi TSJ, Razazpour F, Behroozibakhsh M. The effect of thermocycling on the degree of conversion and mechanical properties of a microhybrid dental resin composite. Restor Dent Endod. 2018;43(2):e26.
  • Azmy E, Al-Kholy MRZ, Fattouh M, Kenawi LMM, Helal MA. Impact of nanoparticles additions on the strength of dental composite resin. Int J Biomater. 2022;2022:1165431.
  • DelPriore K, Ismail HS, Morrow BR, Hill AE, Garcia-Godoy F. Comparative evaluation of subgingival scaling and polishing techniques on dental material surface roughness. Am J Dent. 2023;36(4):207–12.
  • Karimzadeh A, Ayatollahi MR, Shirazi HA. Mechanical properties of a dental nano-composite in moist media determined by nano-scale measurement. International Journal of Materials, Mechanics and Manufacturing. 2014;2(1):67–72.
  • Erdemir U, Sancakli HS, Yildiz E. The effect of one-step and multi-step polishing systems on the surface roughness and microhardness of novel resin composites. Eur J Dent. 2012;6(02):198–205.
  • Martos J, Osinaga PWR, Oliveira E de, Castro LAS de. Hydrolytic degradation of composite resins: effects on the microhardness. Materials Research. 2003;6:599–604.
  • Hubbezoglu I, Bolayir G, Dogan OM, Dogan A, ÖZER A, Bek B. Microhardness evaluation of resin composites polymerized by three different light sources. Dent Mater J. 2007;26(6):845–53.
  • Wei Y jie, Silikas N, Zhang Z ting, Watts DC. Diffusion and concurrent solubility of self-adhering and new resin–matrix composites during water sorption/desorption cycles. Dental Materials. 2011;27(2):197–205.
  • Al-Odayni AB, Saeed WS, Khan R, Al-Kahtani A, Aouak T, Almutairi K, et al. Viscosity, Degree of Polymerization, Water Uptake, and Water Solubility Studies on Experimental Dichloro-BisGMA-Based Dental Composites. Applied Sciences. 2021;11(8):3577.
  • Saikaew P, Phimolthares P, Phitakthanaakul P, Sirikul P, Mekrakseree S, Panpisut P. Effects of color modifier on degree of monomer conversion, biaxial flexural strength, surface microhardness, and water sorption/solubility of resin composites. Polymers (Basel). 2021;13(22):3902.
  • Sandner B, Baudach S, Davy KWM et al, Braden M, Clarke RL. Synthesis of BISGMA derivatives, properties of their polymers and composites. J Mater Sci Mater Med. 1997;8(1):39–44.
  • Kakaboura A, Fragouli M, Rahiotis C, Silikas N. Evaluation of surface characteristics of dental composites using profilometry, scanning electron, atomic force microscopy and gloss-meter. J Mater Sci Mater Med. 2007;18:155–63.
  • Barutcugil Ç, Kürklü D, Barutcugil K, HARORLI O. Beyazlatıcı ağız gargaralarının kompozit rezinin yüzey pürüzlülüğü üzerine etkilerinin incelenmesi. Atatürk Üniversitesi Diş Hekimliği Fakültesi Dergisi. 2014;24(1):33–8.
  • Mehmet B, Öztaş N. Cam iyonomer içerikli farklı restoratif materyallerin yüzey pürüzlülüklerinin değerlendirilmesi. Acta Odontologica Turcica. 2013;30(1):13–7.
  • Bollenl CML, Lambrechts P, Quirynen M. Comparison of surface roughness of oral hard materials to the threshold surface roughness for bacterial plaque retention: a review of the literature. Dental materials. 1997;13(4):258–69.
  • Özcan S, Şahin FÜ, Özgür U, Topuz Ö. Bitirme ve parlatma işlemlerinin farklı kompozit rezinlerin yüzey özellikleri üzerine etkileri. Gazi Üniversitesi Diş Hekimliği Fakültesi Dergisi. 2012;29(3):173–7.
  • Nasoohi N, Hoorizad M, Tabatabaei SF. Effects of wet and dry finishing and polishing on surface roughness and microhardness of composite resins. J Dent (Tehran). 2017;14(2):69.
  • Schmitt VL, Puppin-Rontani RM, Naufel FS, Nahsan FPS, Alexandre Coelho Sinhoreti M, Baseggio W. Effect of the polishing procedures on color stability and surface roughness of composite resins. Int Sch Res Notices. 2011;2011.
  • Lempel E, Tóth Á, Fábián T, Krajczár K, Szalma J. Retrospective evaluation of posterior direct composite restorations: 10-year findings. Dental Materials. 2015;31(2):115–22.
  • van Dijken JW V. A 6-year prospective evaluation of a one-step HEMA-free self-etching adhesive in Class II restorations. Dental Materials. 2013;29(11):1116–22.
  • Jones CS, Billington RW, Pearson GJ. The in vivo perception of roughness of restorations. Br Dent J. 2004;196(1):42–5.
  • Beyth N, Bahir R, Matalon S, Domb AJ, Weiss EI. Streptococcus mutans biofilm changes surface-topography of resin composites. dental materials. 2008;24(6):732–6.
Year 2023, Volume: 1 Issue: 3, 58 - 64, 20.12.2023

Abstract

Supporting Institution

Yoktur

Project Number

Yoktur

Thanks

Yoktur

References

  • Kaizer MR, de Oliveira-Ogliari A, Cenci MS, Opdam NJM, Moraes RR. Do nanofill or submicron composites show improved smoothness and gloss? A systematic review of in vitro studies. Dental Materials. 2014;30(4):e41–78.
  • Nimet Ü, Ülkü SG. Son 10 yılda kompozit rezin restorasyonlar: in vivo ve in vitro çalışmalarla bir derleme. Necmettin Erbakan Üniversitesi Diş Hekimliği Dergisi. 2020;2(3):124–45.
  • Hervás García A, Lozano M, Cabanes Vila J, Barjau Escribano A, Fos Galve P. Composite resins: a review of the materials and clinical indications. 2006;11(2):E215–20.
  • Santerre JP, Shajii L, Leung BW. Relation of dental composite formulations to their degradation and the release of hydrolyzed polymeric-resin-derived products. Critical Reviews in Oral Biology & Medicine. 2001;12(2):136–51.
  • Sideridou ID, Karabela MM. Effect of the amount of 3-methacyloxypropyltrimethoxysilane coupling agent on physical properties of dental resin nanocomposites. Dental Materials. 2009;25(11):1315–24.
  • Hosseinalipour M, Javadpour J, Rezaie H, Dadras T, Hayati AN. Investigation of mechanical properties of experimental Bis‐GMA/TEGDMA dental composite resins containing various mass fractions of silica nanoparticles. Journal of Prosthodontics: Implant, Esthetic and Reconstructive Dentistry. 2010;19(2):112–7.
  • Ritter A V. Sturdevant’s art & science of operative dentistry-e-book. Elsevier Health Sciences; 2017. 470–471 p.
  • Berto-Inga J, Santander-Rengifo F, Ladera-Castañeda M, López-Gurreonero C, Pérez-Vargas AC, Cornejo-Pinto A, et al. Surface Microhardness of Bulk-Fill Resin Composites Handled With Gloves. Int Dent J. 2023;73(4):489–95.
  • Özyurt E. Güncel Rezin Kompozit Materyallerin Fiziksel ve Optik Özelliklerinin Değerlendirilmesi. Selcuk Dental Journal. 2023;10(1):7–11.
  • Bilgili D, Dündar A, Barutçugil Ç, Öcal İB. Farkli cila sistemlerinin kompozit rezinlerin yüzey pürüzlülükleri üzerine etkisi. 7tepe Klinik Dergisi. 2020;16(2):147–53.
  • Sideridou I, Tserki V, Papanastasiou G. Study of water sorption, solubility and modulus of elasticity of light-cured dimethacrylate-based dental resins. Biomaterials. 2003;24(4):655–65.
  • Szalewski L, Wójcik D, Sofińska-Chmiel W, Kuśmierz M, Różyło-Kalinowska I. How the duration and mode of photopolymerization affect the mechanical properties of a dental composite resin. Materials. 2022;16(1):113.
  • Özmen S, Bengü D, ŞenolL AA, Korkut B, Tarçın B, Atalı PY. Tarihi geçmiş kompozit rezinleri kullanmak mümkün mü?: FTIR analizi. Istanbul Kent University Journal of Health Sciences. 2023;2(1):5–11.
  • Cazzaniga G, Ottobelli M, Ionescu A, Garcia-Godoy F, Brambilla E. Surface properties of resin-based composite materials and biofilm formation: A review of the current literature. Am J Dent. 2015;28(6):311–20.
  • Marovic D, Panduric V, Tarle Z, Ristic M, Sariri K, Demoli N, et al. Degree of conversion and microhardness of dental composite resin materials. J Mol Struct. 2013;1044:299–302.
  • Rodrigues-Junior SA, Chemin P, Piaia PP, Ferracane JL. Surface roughness and gloss of actual composites as polished with different polishing systems. Oper Dent. 2015;40(4):418–29.
  • Tofan SA, Todor L, Cosoroabă R, Tănase AD, Todor SA, Popovici RA. Dental Biomaterials in Dental Filling: Why and How to Use? Research and Clinical Medicine Journal. 2021;5(3):11–5.
  • Torres CRG. Modern operative dentistry: Principles for clinical practice. Springer Nature; 2019.
  • Craig RG, Powers JM, Sakaguchi RL. Craig’s restorative dental materials. 13th ed. Mechanical properties. St. Louis: Mosby; 2006. 166–170 p.
  • Caprili S, Mattei F, Mazzatura I, Ferrari F, Gammino M, Mariscotti M, et al. Evaluation of mechanical characteristics of steel bars by non-destructive Vickers micro-hardness tests. Procedia Structural Integrity. 2023;44:886–93.
  • Filija E, Šalinović I. Microhardness testing: can we measure the repair of demineralized lesion? Sonda: List studenata Stomatološkog fakulteta Sveučilišta u Zagrebu. 2022;21(43):44–7.
  • ISO B. 4049: 2019; Dentistry—Polymer-Based Restorative Materials [Internet]. British Standard: London, UK. 2019 [cited 2023 Aug 25]. Available from: https://www.iso.org/standard/67596.html.
  • Çetin AR, Hataysal AE, Aktaş B. Yeni iki tip kompozit materyalin mekanik özelliklerinin karşılaştırılması. Selcuk Dental Journal. 2018;5(3):194–202.
  • Ghavami-Lahiji M, Firouzmanesh M, Bagheri H, Kashi TSJ, Razazpour F, Behroozibakhsh M. The effect of thermocycling on the degree of conversion and mechanical properties of a microhybrid dental resin composite. Restor Dent Endod. 2018;43(2):e26.
  • Azmy E, Al-Kholy MRZ, Fattouh M, Kenawi LMM, Helal MA. Impact of nanoparticles additions on the strength of dental composite resin. Int J Biomater. 2022;2022:1165431.
  • DelPriore K, Ismail HS, Morrow BR, Hill AE, Garcia-Godoy F. Comparative evaluation of subgingival scaling and polishing techniques on dental material surface roughness. Am J Dent. 2023;36(4):207–12.
  • Karimzadeh A, Ayatollahi MR, Shirazi HA. Mechanical properties of a dental nano-composite in moist media determined by nano-scale measurement. International Journal of Materials, Mechanics and Manufacturing. 2014;2(1):67–72.
  • Erdemir U, Sancakli HS, Yildiz E. The effect of one-step and multi-step polishing systems on the surface roughness and microhardness of novel resin composites. Eur J Dent. 2012;6(02):198–205.
  • Martos J, Osinaga PWR, Oliveira E de, Castro LAS de. Hydrolytic degradation of composite resins: effects on the microhardness. Materials Research. 2003;6:599–604.
  • Hubbezoglu I, Bolayir G, Dogan OM, Dogan A, ÖZER A, Bek B. Microhardness evaluation of resin composites polymerized by three different light sources. Dent Mater J. 2007;26(6):845–53.
  • Wei Y jie, Silikas N, Zhang Z ting, Watts DC. Diffusion and concurrent solubility of self-adhering and new resin–matrix composites during water sorption/desorption cycles. Dental Materials. 2011;27(2):197–205.
  • Al-Odayni AB, Saeed WS, Khan R, Al-Kahtani A, Aouak T, Almutairi K, et al. Viscosity, Degree of Polymerization, Water Uptake, and Water Solubility Studies on Experimental Dichloro-BisGMA-Based Dental Composites. Applied Sciences. 2021;11(8):3577.
  • Saikaew P, Phimolthares P, Phitakthanaakul P, Sirikul P, Mekrakseree S, Panpisut P. Effects of color modifier on degree of monomer conversion, biaxial flexural strength, surface microhardness, and water sorption/solubility of resin composites. Polymers (Basel). 2021;13(22):3902.
  • Sandner B, Baudach S, Davy KWM et al, Braden M, Clarke RL. Synthesis of BISGMA derivatives, properties of their polymers and composites. J Mater Sci Mater Med. 1997;8(1):39–44.
  • Kakaboura A, Fragouli M, Rahiotis C, Silikas N. Evaluation of surface characteristics of dental composites using profilometry, scanning electron, atomic force microscopy and gloss-meter. J Mater Sci Mater Med. 2007;18:155–63.
  • Barutcugil Ç, Kürklü D, Barutcugil K, HARORLI O. Beyazlatıcı ağız gargaralarının kompozit rezinin yüzey pürüzlülüğü üzerine etkilerinin incelenmesi. Atatürk Üniversitesi Diş Hekimliği Fakültesi Dergisi. 2014;24(1):33–8.
  • Mehmet B, Öztaş N. Cam iyonomer içerikli farklı restoratif materyallerin yüzey pürüzlülüklerinin değerlendirilmesi. Acta Odontologica Turcica. 2013;30(1):13–7.
  • Bollenl CML, Lambrechts P, Quirynen M. Comparison of surface roughness of oral hard materials to the threshold surface roughness for bacterial plaque retention: a review of the literature. Dental materials. 1997;13(4):258–69.
  • Özcan S, Şahin FÜ, Özgür U, Topuz Ö. Bitirme ve parlatma işlemlerinin farklı kompozit rezinlerin yüzey özellikleri üzerine etkileri. Gazi Üniversitesi Diş Hekimliği Fakültesi Dergisi. 2012;29(3):173–7.
  • Nasoohi N, Hoorizad M, Tabatabaei SF. Effects of wet and dry finishing and polishing on surface roughness and microhardness of composite resins. J Dent (Tehran). 2017;14(2):69.
  • Schmitt VL, Puppin-Rontani RM, Naufel FS, Nahsan FPS, Alexandre Coelho Sinhoreti M, Baseggio W. Effect of the polishing procedures on color stability and surface roughness of composite resins. Int Sch Res Notices. 2011;2011.
  • Lempel E, Tóth Á, Fábián T, Krajczár K, Szalma J. Retrospective evaluation of posterior direct composite restorations: 10-year findings. Dental Materials. 2015;31(2):115–22.
  • van Dijken JW V. A 6-year prospective evaluation of a one-step HEMA-free self-etching adhesive in Class II restorations. Dental Materials. 2013;29(11):1116–22.
  • Jones CS, Billington RW, Pearson GJ. The in vivo perception of roughness of restorations. Br Dent J. 2004;196(1):42–5.
  • Beyth N, Bahir R, Matalon S, Domb AJ, Weiss EI. Streptococcus mutans biofilm changes surface-topography of resin composites. dental materials. 2008;24(6):732–6.
There are 45 citations in total.

Details

Primary Language English
Subjects Restorative Dentistry
Journal Section Research Articles
Authors

Merve Yıldırım Üçüncü 0000-0001-8136-230X

Musa Kazım Üçüncü 0000-0002-2352-8532

Project Number Yoktur
Publication Date December 20, 2023
Submission Date August 25, 2023
Published in Issue Year 2023 Volume: 1 Issue: 3

Cite

Vancouver Yıldırım Üçüncü M, Üçüncü MK. Comparison of the Mechanical Properties of Various Microhybrid Dental Composites. EDR. 2023;1(3):58-64.