PRODUCTION OF PROPOLIS POWDER BY VACUUM DRYING AND SOME PROPERTIES OF THE POWDER

Year 2023, Volume: 48 Issue: 6, 1292 - 1303, 15.12.2023

Ceren Mutlu

https://doi.org/10.15237/gida.GD23109

Abstract

The aim of this study was to determine some properties of propolis powder produced by vacuum-drying of propolis 70% of ethanol extract with gum arabic. The total phenolic and flavonoid contents of sample were 5.65 g GAE/100 g and 1.08 g QE/100 g, respectively, and these results were lower than the those of raw propolis. Furthermore, TEAC and CUPRAC results of sample were 541.54 and 462.47 µmol TE/g, respectively. Hausner ratio and Carr index values were 1.33 and 24.65%, respectively, and flowability was passable. It was concluded that, moisture adsorption of propolis powder showed Type 2 characteristics, monolayer moisture content was ≤5.44 g/100 g, and BET, Halsey and Kuhn models had a good fit to the moisture adsorption of propolis powder at 25°C. As a result, it was evaluated that produced propolis powder contains bioactive components and can be safely stored at a moisture content lower than 5.44 g/100 g.

Keywords

Propolis, Carr index, phenolic, adsorption, Halsey

VAKUM KURUTMA YÖNTEMİ İLE PROPOLİS TOZU ÜRETİMİ VE TOZUN BAZI ÖZELLİKLERİ

Abstract

Araştırmada %70 etanol ile ekstrakte edilmiş propolisin Arap zamkı ilavesiyle ve vakumda kurutulmasıyla üretilen propolis tozunun bazı özelliklerinin belirlenmesi amaçlanmıştır. Propolis tozunun toplam fenolik madde ve flavonoid içerikleri sırasıyla 5.65 g gallik asit eşdeğeri/100 g ve 1.08 g kuersetin eşdeğeri/100 g olarak belirlenmiş ve bu sonuçların ham propolis örneğine ait sonuçlardan daha düşük olduğu tespit edilmiştir. Ayrıca üretilen tozun TEAC ve CUPRAC analiz sonuçları sırasıyla 541.54 ve 462.47 µmol Troloks eşdeğeri/g olarak bulunmuştur. Hausner oranı ve Carr indeksi değerleri sırasıyla 1.33 ve %24.65 olarak belirlenmiş olup, toz örneğin akışkanlığının orta düzeyde olduğu değerlendirilmiştir. Propolis tozunun nem adsorpsiyonunun Tip 2 özellik gösterdiği, tek tabaka su içeriğinin ≤5.44 g/100 g olduğu ve BET, Halsey ve Kuhn modellerinin 25°C sıcaklıkta nem adsorpsiyonunu daha iyi temsil ettiği belirlenmiştir. Sonuç olarak üretilen propolis tozunun biyoaktif bileşenler içerdiği ve 5.44 g/100 g değerinden daha düşük nem içeriğinde güvenli olarak muhafaza edilebileceği değerIendirilmiştir.

Keywords

Propolis, Carr indeks, fenolik, adsorpsiyon, Halsey

Ethical Statement

Araştırmada herhangi bir canlı kullanılmadığından etik kurul onayına ihtiyaç bulunmamaktadır.

Supporting Institution

Destekleyen bir kurum bulunmamaktadır.

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