Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method

Year 2023, Volume: 6 Issue: 1, 83 - 86, 21.06.2023

Tankut Ateş , Niyazi Bulut , Omer Kaygılı , Serhat Keser

https://doi.org/10.54565/jphcfum.1287104

Abstract

In this study, the effects of the duration of ultrasonication for Pr-doped hydroxyapatite (HA) were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared (FT-IR) analyses. 0.25at.%Pr-containing HA samples were prepared by the ultrasonic-assisted wet chemical route using different ultrasonication times of 0, 30, 60, 90, and 120 min. The formation of the HA phase was confirmed by the FT-IR and XRD data for each sample. The morphology was significantly affected by the duration of ultrasonication. Compared to the untreated sample, remarkable decreases in both the crystallite size and the crystallinity were observed with the duration of ultrasonication.

Keywords

Bioceramics, X-ray techniques, Hydroxyapatite

Supporting Institution

Unit of Scientific Research Projects of Firat University (FUBAP)

Project Number

FF.23.12 and FF.23.13

Thanks

This work was supported by the Management Unit of Scientific Research Projects of Firat University (FUBAP) (Project Numbers: FF.23.12 and FF.23.13).

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