Fe ve Ti katkılı Çift Fazlı Kalsiyum Fosfatların Sentez ve Karakterizasyonu

Year 2021, Volume: 10 Issue: 2, 89 - 94, 31.12.2021

Tankut Ateş , Turan Ince , Serdar Acar , Omer Kaygılı , Niyazi Bulut , Serhat Keser , Süleyman Köytepe

https://doi.org/10.46810/tdfd.885177

Abstract

Bu çalışmada, Ti katkısının Fe esaslı çift fazlı kalsiyum fosfat malzemelerinin yapısal, morfolojik ve termal özellikleri üzerine etkileri araştırılmıştır. X-ışını kırınımı (XRD) analizi, üretilen numunelerin hem hidroksiapatit (HAp) hem de beta trikalsiyum fosfat (β-TCP) fazlarına sahip olduğunu doğrulamaktadır. Ayrıca, Ti katkısındaki artışla β-TCP fazının miktarının arttığı görülmektedir. Fourier dönüşümlü kızılötesi (FTIR) spektroskopisi sonuçları, numunelerdeki karakteristik fonksiyonel grupların varlığını doğrulamaktadır. Ti miktarı morfolojiyi etkilemektedir. Numunelerin ısıl davranışları birbirine benzerdir ve oda sıcaklığından 1000 °C’ye kadar tüm numuneler termal olarak kararlıdırlar. Bu sıcaklık aralığında numunelerdeki kütle kayıpları % 1,63’e eşit veya altındadır.

Keywords

Hidroksiapatit, Beta trikalsiyum fosfat (β-TCP), X-ışını kırınımı (XRD), Morfoloji

Supporting Institution

Fırat Üniversitesi Bilimsel Araştırma Projeleri (FÜBAP) Birimi

Project Number

FF.20.16

Thanks

Bu çalışma, Fırat Üniversitesi Bilimsel Araştırma Projeleri (FÜBAP) tarafından FF.20.16 proje kapsamında desteklenmiştir.

Synthesis and Characterization of Fe and Ti Doped Biphasic Calcium Phosphates

Abstract

In this study, the effects of Ti doping on the structural, morphological, and thermal properties of the Fe-based biphasic calcium phosphates have been investigated. X-ray diffraction (XRD) analysis has verified that the-as produced samples have both hydroxyapatite (HAp) and beta-tricalcium phosphate (β-TCP) phases. Besides, it has been seen that the amount of β-TCP phase increases with the increase in Ti doping. Fourier transform infrared (FTIR) spectroscopy results have verified the existence of the characteristic functional groups in the samples. Ti amount affects the morphology. The thermal behaviors of the samples are similar to each other, and all the samples are thermally stable from room temperature to 1000 °C. In this temperature range, the mass losses in the samples are equal to or smaller than 1.63 %.

Keywords

Hydroxyapatite, Beta tricalcium phosphate (β-TCP), X-ray diffraction (XRD), Morphology

Project Number

FF.20.16

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