Year 2018,
Volume: 2 Issue: 1, 1 - 6, 01.01.2018
Canan Aksu Canbay
,
Himdad İbrahim Mustafa
İskender Özkul
References
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CHARACTERIZATION OF HYDROTHERMALLY SYNTHESISED HYDROXYAPATITE BIOCERAMIC
Year 2018,
Volume: 2 Issue: 1, 1 - 6, 01.01.2018
Canan Aksu Canbay
,
Himdad İbrahim Mustafa
İskender Özkul
Abstract
In this study, hydroxyapatite (HAP) was synthesized by hydrothermal method. The structural analysis, thermal analysis and electrical characteristics of HAP sample have been investigated. The structural analysis was performed to determine the crystal structure and to observe the surface morphology of the sample. The thermal analysis was made from room temperature to 925 ˚C, to determine the mass loss according to temperature and phase transitions or decomposition in the sample and also TG-DTA analysis was done to determine the thermal stability. The compositional analysis was done by EDX. I-V analysis was made to calculate the electrical conductivity value of the sample and electrical conductivity of the sample was obtained to be 1.2x10-10 S/cm.
References
- Al-Hazmi, F. E. (2016). "Synthesis and electrical properties of Bi doped hydroxyapatite ceramics." Journal of Alloys and Compounds, Vol. 665, pp. 119-123.
- Badran, H., I. Yahia, M. S. Hamdy and N. Awwad (2017). "Lithium-doped hydroxyapatite nano-composites: Synthesis, characterization, gamma attenuation coefficient and dielectric properties." Radiation Physics and Chemistry, Vol. 130, pp. 85-91.
- Brown, P. W. and B. Constantz (1994). Hydroxyapatite and related materials. CRC press, USA.
- Gümüşderelioğlu, M. (2002). "Biyomalzemeler." Bilim ve Teknik Dergisi, TÜBİTAK, Temmuz özel sayısı.
- Hench, L. L. and J. Wilson (1993). An introduction to bioceramics. USA, World scientific.
- Jagadale, P. N., P. P. Jagtap, M. G. Joshi and S. R. Bamane (2016). "A prototype synthesis and characterization of hydroxyapatite bioceramics nanocrystallites." Advanced Materials Letters, Vol. 7, No. 4, pp. 325-329.
- Orlovskii, V., V. Komlev and S. Barinov (2002). "Hydroxyapatite and hydroxyapatite-based ceramics." Inorganic Materials, Vol. 38, No. 10, pp. 973-984.
- Padiyan, D. P., A. Marikani and K. Murali (2003). "Influence of thickness and substrate temperature on electrical and photoelectrical properties of vacuumdeposited CdSe thin films." Materials Chemistry and Physics, Vol. 78, No. 1, pp. 51-58.
- Park, J. B. and J. D. Bronzino (2002). Biomaterials: principles and applications, crc press, USA.
- Pasinli, A. (2004). "Biyomedikal uygulamalarda kullanılan biyomalzemeler." Makine Teknolojileri Elektronik Dergisi, Vol. 4, pp. 25-34.
- Sadat-Shojai, M., M.-T. Khorasani, E. DinpanahKhoshdargi and A. Jamshidi (2013). "Synthesis methods for nanosized hydroxyapatite with diverse structures." Acta biomaterialia, Vol. 9, No. 8, pp. 7591-7621.
- Sato, M., M. A. Sambito, A. Aslani, N. M. Kalkhoran, E. B. Slamovich and T. J. Webster (2006). "Increased osteoblast functions on undoped and yttrium-doped nanocrystalline hydroxyapatite coatings on titanium." Biomaterials, Vol. 27, No. 11, pp. 2358-2369.
- Singh, R. and J. S. Sidhu (2014). "Synthesis and Characterization of Biomaterial Hydroxyapatite." International Journal of Engineering Sciences & Research Technology Vol. 3, No. 8, pp. 744-758.
- Stanić, V., S. Dimitrijević, J. Antić-Stanković, M. Mitrić, B. Jokić, I. B. Plećaš and S. Raičević (2010). "Synthesis, characterization and antimicrobial activity of copper and zinc-doped hydroxyapatite nanopowders." Applied Surface Science, Vol. 256, No. 20, pp. 6083-6089.
- Zhang, C., C. Li, S. Huang, Z. Hou, Z. Cheng, P. Yang, C. Peng and J. Lin (2010). "Self-activated luminescent and mesoporous strontium hydroxyapatite nanorods for drug delivery." Biomaterials, Vol. 31, No. 12, pp. 3374-3383.
- Zhang, X. (2007). Preparation and characterization of calcium phosphate ceramics and composites as bone substitutes. University of California, USA.