PİRİNA YAĞININ ÖĞÜTME YARDIMCISI OLARAK KULLANABİLİRLİĞİNİN ARAŞTIRILMASI
Yıl 2021,
, 189 - 201, 31.08.2021
Serkan Çayırlı
,
Hasan Serkan Gökçen
,
Nuri Yüce
Obaidullah Elchi
Öz
Bu çalışmada, kalsitin kuru mikronize boyutlara karıştırmalı bilyalı değirmende öğütülmesinde pirina yağının öğütme yardımcısı olarak kullanılabilirliği araştırılmıştır. Bu amaçla doğrultusunda ilk aşamada farklı stres yoğunlukları oluşturularak optimum öğütme koşulları belirlenmiştir. İkinci aşamada ise pirina yağının kullanılabilirliği araştırılmış ve saf bir öğütme yardımcısı olan trietanolamin ile karşılaştırılmıştır. Deneysel sonuçlar öğütme yardımcısı miktarı, enerji tüketime ve tane boyutu göz önünde bulundurularak değerlendirilmiştir. Elde edilen sonuçlara göre optimum stres yoğunluğu aralığı 500 kJ/kg ve 1000 kJ/kg enerji seviyelerinde yaklaşık 1-2*10-3 Nm olarak belirlenmiştir. 2000 kJ/kg enerji seviyesinde TEA ve pirina yağı kullanımı ile 4 µm ve altı tane boyutuna sahip ürünler üretilebilmiştir. Pirina yağı kullanımı ile özellikle ileri enerji seviyelerinde (1000 kJ/kg ve 2000 kJ/kg) TEA’ya yakın tane boyutları elde edilmiştir.
Destekleyen Kurum
Türkiye Bilimsel ve Teknolojik Araştırma Kurumu (TÜBİTAK)
Teşekkür
Yazarlar, çalışmayı 119M216 no’lu proje kapsamında maddi olarak destekleyen Türkiye Bilimsel ve Teknolojik Araştırma Kurumu (TÜBİTAK)’na, deneysel çalışmalarda kullanılan malzemenin temini için MİKRON’S Mikronize Mineral End. ve Tic. A.Ş.’ ye ve kullanılan pirina yağının temini için Dalan Yağ Endüstri A.Ş.’ye teşekkürlerini sunar.
Kaynakça
- Akar, C., ve Canbaz, M. (2016). Effect of molasses as an admixture on concrete durability. Journal of Cleaner Production, 112, 2374-2380. doi:https://doi.org/10.1016/j.jclepro.2015.09.081
- Altun, O., Benzer, H., Toprak, A., ve Enderle, U. (2015). Utilization of grinding aids in dry horizontal stirred milling. Powder Technology, 286, 610-615. doi:https://doi.org/10.1016/j.powtec.2015.09.001
- Austin, L. G., Klimpel, R. R., ve Luckie, P. T. (1984). Process engineering of size reduction: Ball milling: Society of Mining Engineers of the AIME.
- Cayirli, S. (2018). Influences of operating parameters on dry ball mill performance. Physicochemical Problems of Mineral Processing, 54. doi:https://doi.org/10.5277/ppmp1876
- Cayirli, S., ve Gokcen, H. (2017). The effect of stirred mill orientation on calcite grinding. Paper presented at the 15th European Symposium on Comminution & Classification/İzmir, Turkey.
- Conway-Baker, J., Barley, R. W., Williams, R. A., Jia, X., Kostuch, J., McLoughlin, B., ve Parker, D. J. (2002). Measurement of the motion of grinding media in a vertically stirred mill using positron emission particle tracking (pept). Minerals Engineering, 15(1-2), 53-59. doi:https://doi.org/10.1016/S0892-6875(01)00199-6
- Çayırlı, S. (2018). Kalsitin dik ve yatay karıştırmalı bilyalı değirmende öğütülmesinde İşlem parametrelerinin etkisinin araştırılması (FEB 2016/23-BAGEP). Erişim adresi: Niğde Ömer Halisdemir Üniversitesi Bilimsel Araştırma Projesi: https://www.ohu.edu.tr/bap
- Çayirli, S., ve Gökçen, H. S. (2018). Kalsitin dik ve yatay karıştırmalı değirmende öğütülmesinde öğütme yardımcısının etkisinin İncelenmesi. Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi. doi:https://doi.org/10.28948/ngumuh.445283
- Dikmen, S., ve Ergün, Ş. (2004). Karıştırmalı bilyalı değirmenler. Madencilik Dergisi, 43(4), 3-15.
- Dombrowe, H., Hoffmann, B., ve Scheibe, W. (1982). Mode of action and possibilities for use of grinding aids. Zement-Kalk-Gips, Edition B, 35(11), 571-580.
- El-Shall, H., ve Somasundaran, P. (1984). Mechanisms of grinding modification by chemical additives: Organic reagents, powder technology 38(3), 267-273. Powder Technology, 38(3),, 267-273.
- Forssberg, E., Wang, Y., ve Persson, H. (1995). Dry fine grinding of dolomite with the sala agitated mill sam 7.5-effects of grinding media and grinding additive. Aufbereitungs-Technik, 36.
- Fuerstenau, D. W. (1995). Grinding aids. KONA Powder and Particle Journal, 13(0), 5-18. doi:https://doi.org/10.14356/kona.1995006
- Gao, X., Yang, Y., ve Deng, H. (2011). Utilization of beet molasses as a grinding aid in blended cements. Construction and Building Materials, 25(9), 3782-3789. doi:https://doi.org/10.1016/j.conbuildmat.2011.04.041
- Gokcen, H. S., Cayirli, S., Ucbas, Y., ve Kayaci, K. (2015). The effect of grinding aids on dry micro fine grinding of feldspar. International Journal of Mineral Processing, 136(Supplement C), 42-44. doi:https://doi.org/10.1016/j.minpro.2014.10.001
- Hasegawa, M., Kimata, M., Shimane, M., Shoji, T., ve Tsuruta, M. (2001). The effect of liquid additives on dry ultrafine grinding of quartz. Powder Technology, 114(1), 145-151. doi:https://doi.org/10.1016/S0032-5910(00)00290-4
- Hasegawa, M., Kimata, M., ve Yaguchi, M. (2006). Effect and behavior of liquid additive molecules in dry ultrafine grinding of limestone [translated]†. KONA Powder and Particle Journal, 24(0), 213-221. doi:https://doi.org/10.14356/kona.2006023
- Jankovic, A. (2003). Variables affecting the fine grinding of minerals using stirred mills. Minerals Engineering, 16(4), 337-345. doi:https://doi.org/10.1016/s0892-6875(03)00007-4
- Kwade, A. (2013). Grinding and dispersing with stirred media mills (3. edition ed.). Braunschweig: iPAT.
- Leoneti, A. B., Aragão-Leoneti, V., ve De Oliveira, S. V. W. B. (2012). Glycerol as a by-product of biodiesel production in brazil: Alternatives for the use of unrefined glycerol. Renewable Energy, 45, 138-145. doi:https://doi.org/10.1016/j.renene.2012.02.032
- Li, H., Jiang, Z., Yang, X., Yu, L., Zhang, G., Wu, J., ve Liu, X. (2015). Sustainable resource opportunity for cane molasses: Use of cane molasses as a grinding aid in the production of portland cement. Journal of Cleaner Production, 93, 56-64. doi:https://doi.org/10.1016/j.jclepro.2015.01.027
- Li, H., Zhao, J., Huang, Y., Jiang, Z., Yang, X., Yang, Z., ve Chen, Q. (2016). Investigation on the potential of waste cooking oil as a grinding aid in portland cement. J Environ Manage, 184(Pt 3), 545-551. doi:https://doi.org/10.1016/j.jenvman.2016.10.027
- Li, L., Feng, Y., Liu, M., ve Zhao, F. (2017). Preparation of grinding aid using waste acid residue from plasticizer plant. IOP Conference Series: Materials Science and Engineering, 230, 012023. doi:https://doi.org/10.1088/1757-899x/230/1/012023
- Li, W., Ma, S., ve Shen, X. (2018). Washington Patent No. 10,077,211. U.S. Patent and Trademark Office.
- Li, Y., Zhu, H., Yang, C., Zhang, Y., Xu, J., ve Lu, M. (2014). Synthesis and super retarding performance in cement production of diethanolamine modified lignin surfactant. Construction and Building Materials, 52, 116-121. doi:https://doi.org/10.1016/j.conbuildmat.2013.09.024
- Locher, F. W., ve Seebach, H. M. v. (1972). Influence of adsorption on industrial grinding. Industrial & Engineering Chemistry Process Design and Development, 11(2), 190-197. doi:https://doi.org/10.1021/i260042a007
- Lowrison, G. C. (1974). Crushing and grinding: The size reduction of solid materials: Butterworths.
- Madlool, N. A., Saidur, R., Hossain, M. S., ve Rahim, N. A. (2011). A critical review on energy use and savings in the cement industries. Renewable and Sustainable Energy Reviews, 15(4), 2042-2060. doi:https://doi.org/10.1016/j.rser.2011.01.005
- Mankosa, M. J., Adel, G. T., ve Yoon, R. H. (1986). Effect of media size in stirred ball mill grinding of coal. Powder Technology, 49(1), 75-82. doi:https://doi.org/10.1016/0032-5910(86)85008-2
- Mende, S., Stenger, F., Peukert, W., ve Schwedes, J. (2004). Production of sub-micron particles by wet comminution in stirred media mills. Journal of Materials Science, 39(16), 5223-5226. doi:https://doi.org/10.1023/B:JMSC.0000039214.12131.58
- Orumwense, O. A., ve Forssberg, E. (1992). Superfine and ultrafine grinding a literature survey. Mineral Processing and Extractive Metallurgy Review, 11(1-2), 107-127. doi:https://doi.org/10.1080/08827509208914216
- Paramasivam, R., ve Vedaraman, R. (1992). Effects of the physical properties of liquid additives on dry grinding. Powder Technology, 70(1), 43-50. doi:https://doi.org/10.1016/0032-5910(92)85052-W
- Prziwara, P., Breitung-Faes, S., ve Kwade, A. (2018). Impact of grinding aids on dry grinding performance, bulk properties and surface energy. Advanced Powder Technology, 29(2), 416-425. doi:https://doi.org/10.1016/j.apt.2017.11.029
- Rácz, Á., ve Csőke, B. (2016). Application of the product related stress model for product dispersity control in dry stirred media milling. International Journal of Mineral Processing, 157, 28-35. doi:http://dx.doi.org/10.1016/j.minpro.2016.09.005
- Sohoni, S., Sridhar, R., ve Mandal, G. (1991). The effect of grinding aids on the fine grinding of limestone, quartz and portland cement clinker. Powder Technology, 67(3), 277-286. doi:https://doi.org/10.1016/0032-5910(91)80109-V
- Toprak, N. A., Altun, O., ve Benzer, A. H. (2018). The effects of grinding aids on modelling of air classification of cement. Construction and Building Materials, 160, 564-573. doi:https://doi.org/10.1016/j.conbuildmat.2017.11.088
- Toraman, O., Çayirli, S., ve Uçurum, M. (2016). The grinding-aids effect of moisture, triethanolamine (tea) and ethylene glycol (eg) on grinding performance and product quality of calcite. International Journal of Engineering Research & Science (IJOER), 2(12), 121-128.
- Uçbaş, Y., Kayacı, K., Gökçen, H. S., ve Çayırlı, S. (2011). Sodyum feldispatın karıştırmalı bilyalı değirmende çok İnce öğütülmesinin porselen seramik karo üretimindeki etkilerinin İncelenmesi (119M114). Erişim adresi: TÜBİTAK: https://app.trdizin.gov.tr/search/projectSearch.xhtml
- Wang, Y., ve Forssberg, E. (2007). Enhancement of energy efficiency for mechanical production of fine and ultra-fine particles in comminution. China Particuology, 5(3), 193-201. doi:https://doi.org/10.1016/j.cpart.2007.04.003
- Zhang, Y., Fei, A., ve Li, D. (2016). Utilization of waste glycerin, industry lignin and cane molasses as grinding aids in blended cement. Construction and Building Materials, 123, 785-791. doi:https://doi.org/10.1016/j.conbuildmat.2016.07.034
THE INVESTIGATION OF USABILITY OF OLIVE POMACE OIL AS A GRINDING AID
Yıl 2021,
, 189 - 201, 31.08.2021
Serkan Çayırlı
,
Hasan Serkan Gökçen
,
Nuri Yüce
Obaidullah Elchi
Kaynakça
- Akar, C., ve Canbaz, M. (2016). Effect of molasses as an admixture on concrete durability. Journal of Cleaner Production, 112, 2374-2380. doi:https://doi.org/10.1016/j.jclepro.2015.09.081
- Altun, O., Benzer, H., Toprak, A., ve Enderle, U. (2015). Utilization of grinding aids in dry horizontal stirred milling. Powder Technology, 286, 610-615. doi:https://doi.org/10.1016/j.powtec.2015.09.001
- Austin, L. G., Klimpel, R. R., ve Luckie, P. T. (1984). Process engineering of size reduction: Ball milling: Society of Mining Engineers of the AIME.
- Cayirli, S. (2018). Influences of operating parameters on dry ball mill performance. Physicochemical Problems of Mineral Processing, 54. doi:https://doi.org/10.5277/ppmp1876
- Cayirli, S., ve Gokcen, H. (2017). The effect of stirred mill orientation on calcite grinding. Paper presented at the 15th European Symposium on Comminution & Classification/İzmir, Turkey.
- Conway-Baker, J., Barley, R. W., Williams, R. A., Jia, X., Kostuch, J., McLoughlin, B., ve Parker, D. J. (2002). Measurement of the motion of grinding media in a vertically stirred mill using positron emission particle tracking (pept). Minerals Engineering, 15(1-2), 53-59. doi:https://doi.org/10.1016/S0892-6875(01)00199-6
- Çayırlı, S. (2018). Kalsitin dik ve yatay karıştırmalı bilyalı değirmende öğütülmesinde İşlem parametrelerinin etkisinin araştırılması (FEB 2016/23-BAGEP). Erişim adresi: Niğde Ömer Halisdemir Üniversitesi Bilimsel Araştırma Projesi: https://www.ohu.edu.tr/bap
- Çayirli, S., ve Gökçen, H. S. (2018). Kalsitin dik ve yatay karıştırmalı değirmende öğütülmesinde öğütme yardımcısının etkisinin İncelenmesi. Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi. doi:https://doi.org/10.28948/ngumuh.445283
- Dikmen, S., ve Ergün, Ş. (2004). Karıştırmalı bilyalı değirmenler. Madencilik Dergisi, 43(4), 3-15.
- Dombrowe, H., Hoffmann, B., ve Scheibe, W. (1982). Mode of action and possibilities for use of grinding aids. Zement-Kalk-Gips, Edition B, 35(11), 571-580.
- El-Shall, H., ve Somasundaran, P. (1984). Mechanisms of grinding modification by chemical additives: Organic reagents, powder technology 38(3), 267-273. Powder Technology, 38(3),, 267-273.
- Forssberg, E., Wang, Y., ve Persson, H. (1995). Dry fine grinding of dolomite with the sala agitated mill sam 7.5-effects of grinding media and grinding additive. Aufbereitungs-Technik, 36.
- Fuerstenau, D. W. (1995). Grinding aids. KONA Powder and Particle Journal, 13(0), 5-18. doi:https://doi.org/10.14356/kona.1995006
- Gao, X., Yang, Y., ve Deng, H. (2011). Utilization of beet molasses as a grinding aid in blended cements. Construction and Building Materials, 25(9), 3782-3789. doi:https://doi.org/10.1016/j.conbuildmat.2011.04.041
- Gokcen, H. S., Cayirli, S., Ucbas, Y., ve Kayaci, K. (2015). The effect of grinding aids on dry micro fine grinding of feldspar. International Journal of Mineral Processing, 136(Supplement C), 42-44. doi:https://doi.org/10.1016/j.minpro.2014.10.001
- Hasegawa, M., Kimata, M., Shimane, M., Shoji, T., ve Tsuruta, M. (2001). The effect of liquid additives on dry ultrafine grinding of quartz. Powder Technology, 114(1), 145-151. doi:https://doi.org/10.1016/S0032-5910(00)00290-4
- Hasegawa, M., Kimata, M., ve Yaguchi, M. (2006). Effect and behavior of liquid additive molecules in dry ultrafine grinding of limestone [translated]†. KONA Powder and Particle Journal, 24(0), 213-221. doi:https://doi.org/10.14356/kona.2006023
- Jankovic, A. (2003). Variables affecting the fine grinding of minerals using stirred mills. Minerals Engineering, 16(4), 337-345. doi:https://doi.org/10.1016/s0892-6875(03)00007-4
- Kwade, A. (2013). Grinding and dispersing with stirred media mills (3. edition ed.). Braunschweig: iPAT.
- Leoneti, A. B., Aragão-Leoneti, V., ve De Oliveira, S. V. W. B. (2012). Glycerol as a by-product of biodiesel production in brazil: Alternatives for the use of unrefined glycerol. Renewable Energy, 45, 138-145. doi:https://doi.org/10.1016/j.renene.2012.02.032
- Li, H., Jiang, Z., Yang, X., Yu, L., Zhang, G., Wu, J., ve Liu, X. (2015). Sustainable resource opportunity for cane molasses: Use of cane molasses as a grinding aid in the production of portland cement. Journal of Cleaner Production, 93, 56-64. doi:https://doi.org/10.1016/j.jclepro.2015.01.027
- Li, H., Zhao, J., Huang, Y., Jiang, Z., Yang, X., Yang, Z., ve Chen, Q. (2016). Investigation on the potential of waste cooking oil as a grinding aid in portland cement. J Environ Manage, 184(Pt 3), 545-551. doi:https://doi.org/10.1016/j.jenvman.2016.10.027
- Li, L., Feng, Y., Liu, M., ve Zhao, F. (2017). Preparation of grinding aid using waste acid residue from plasticizer plant. IOP Conference Series: Materials Science and Engineering, 230, 012023. doi:https://doi.org/10.1088/1757-899x/230/1/012023
- Li, W., Ma, S., ve Shen, X. (2018). Washington Patent No. 10,077,211. U.S. Patent and Trademark Office.
- Li, Y., Zhu, H., Yang, C., Zhang, Y., Xu, J., ve Lu, M. (2014). Synthesis and super retarding performance in cement production of diethanolamine modified lignin surfactant. Construction and Building Materials, 52, 116-121. doi:https://doi.org/10.1016/j.conbuildmat.2013.09.024
- Locher, F. W., ve Seebach, H. M. v. (1972). Influence of adsorption on industrial grinding. Industrial & Engineering Chemistry Process Design and Development, 11(2), 190-197. doi:https://doi.org/10.1021/i260042a007
- Lowrison, G. C. (1974). Crushing and grinding: The size reduction of solid materials: Butterworths.
- Madlool, N. A., Saidur, R., Hossain, M. S., ve Rahim, N. A. (2011). A critical review on energy use and savings in the cement industries. Renewable and Sustainable Energy Reviews, 15(4), 2042-2060. doi:https://doi.org/10.1016/j.rser.2011.01.005
- Mankosa, M. J., Adel, G. T., ve Yoon, R. H. (1986). Effect of media size in stirred ball mill grinding of coal. Powder Technology, 49(1), 75-82. doi:https://doi.org/10.1016/0032-5910(86)85008-2
- Mende, S., Stenger, F., Peukert, W., ve Schwedes, J. (2004). Production of sub-micron particles by wet comminution in stirred media mills. Journal of Materials Science, 39(16), 5223-5226. doi:https://doi.org/10.1023/B:JMSC.0000039214.12131.58
- Orumwense, O. A., ve Forssberg, E. (1992). Superfine and ultrafine grinding a literature survey. Mineral Processing and Extractive Metallurgy Review, 11(1-2), 107-127. doi:https://doi.org/10.1080/08827509208914216
- Paramasivam, R., ve Vedaraman, R. (1992). Effects of the physical properties of liquid additives on dry grinding. Powder Technology, 70(1), 43-50. doi:https://doi.org/10.1016/0032-5910(92)85052-W
- Prziwara, P., Breitung-Faes, S., ve Kwade, A. (2018). Impact of grinding aids on dry grinding performance, bulk properties and surface energy. Advanced Powder Technology, 29(2), 416-425. doi:https://doi.org/10.1016/j.apt.2017.11.029
- Rácz, Á., ve Csőke, B. (2016). Application of the product related stress model for product dispersity control in dry stirred media milling. International Journal of Mineral Processing, 157, 28-35. doi:http://dx.doi.org/10.1016/j.minpro.2016.09.005
- Sohoni, S., Sridhar, R., ve Mandal, G. (1991). The effect of grinding aids on the fine grinding of limestone, quartz and portland cement clinker. Powder Technology, 67(3), 277-286. doi:https://doi.org/10.1016/0032-5910(91)80109-V
- Toprak, N. A., Altun, O., ve Benzer, A. H. (2018). The effects of grinding aids on modelling of air classification of cement. Construction and Building Materials, 160, 564-573. doi:https://doi.org/10.1016/j.conbuildmat.2017.11.088
- Toraman, O., Çayirli, S., ve Uçurum, M. (2016). The grinding-aids effect of moisture, triethanolamine (tea) and ethylene glycol (eg) on grinding performance and product quality of calcite. International Journal of Engineering Research & Science (IJOER), 2(12), 121-128.
- Uçbaş, Y., Kayacı, K., Gökçen, H. S., ve Çayırlı, S. (2011). Sodyum feldispatın karıştırmalı bilyalı değirmende çok İnce öğütülmesinin porselen seramik karo üretimindeki etkilerinin İncelenmesi (119M114). Erişim adresi: TÜBİTAK: https://app.trdizin.gov.tr/search/projectSearch.xhtml
- Wang, Y., ve Forssberg, E. (2007). Enhancement of energy efficiency for mechanical production of fine and ultra-fine particles in comminution. China Particuology, 5(3), 193-201. doi:https://doi.org/10.1016/j.cpart.2007.04.003
- Zhang, Y., Fei, A., ve Li, D. (2016). Utilization of waste glycerin, industry lignin and cane molasses as grinding aids in blended cement. Construction and Building Materials, 123, 785-791. doi:https://doi.org/10.1016/j.conbuildmat.2016.07.034