Nanokompozitlerin Grafen ve Grafen Oksit ile Üretimi ve Karakterizasyonunun İncelenmesi

Yıl 2022, Cilt: 27 Sayı: 3, 1221 - 1234, 31.12.2022

Nihayet Koçyigit

https://doi.org/10.17482/uumfd.1100896

Öz

Bu çalışmanın amacı, epoksi ve CF matrislerine G ve GO ekleyerek G/epoksi, GO/epoksi, G/CFRP, GO/CFRP nanokompozitlerini elde etmek ve bu nanokompozitlerin çekme mukavemeti üzerine G ve GO'nun etkisini araştırmaktır. Bu amaçla, polimer matrislerde G homojen olarak dağılmadığından, G hummers yöntemiyle GO'ya dönüştürülmüş ve elde edilen GO'nun karakterizasyon analizi yapılmıştır. SEM, EDX, FTIR, X-RD analiz sonuçları, GO'nun başarıyla elde edildiğini göstermiştir. Daha sonra epoksi ve CFRP'ye %0,1, %0,2 ve %0,3 oranında G ve GO eklenmiş ve G/epoksi, GO/epoksi, G/CFRP, GO/CFRP nanokompozitleri elde edilmiştir. G ve GO'nun bu nanokompozitlerin çekme mukavemeti üzerindeki etkisini karşılaştırmak için çekme testi uygulanmiştir. En iyi sonuç %0,2 oranında G ve GO ilavesi ile elde edilmiş ve GO'nun çekme mukavemeti üzerindeki etkisinin G'ye göre daha iyi olduğu gözlemlenmiştir.

Anahtar Kelimeler

Hummers metodu, grafen, grafen oksit, CFRP, nanokompozit

PRODUCTION AND CHARACTERIZATION OF NANOCOMPOSITES WITH GRAPHENE AND GRAPHENE OXIDE

Öz

The aim of this study was to i.) obtain Graphene (G)/epoxy, Graphene Oxide (GO)/epoxy, G/carbon fiber reinforced plastic (CFRP), GO/CFRP nanocomposites by G and GO addition to epoxy and CF matrices and ii.) investigate the effect of G and GO addition on tensile strength of the nanocomposites produced. The graphene was not homogeneously distributed in polymer matrices; therefore, the G was converted into the GO using hummers method. The characterization GO was carried out by SEM, EDX, FTIR and X-RD analysis, which confirmed the successful production of the GO. The G/epoxy, GO/epoxy, G/CFRP and GO/CFRP nanocomposites were obtained by adding G and GO to epoxy and CF at a rate of 0.1, 0.2, and 0.3%. The effect of G and GO on tensile strength of the nanocomposites was determined using a tensile test. The addition of G and GO at 0.2% rate yielded the best results. The effect of GO on tensile strength was better compared to that of the G.

Anahtar Kelimeler

Hummers Method, Graphene, Graphene Oxide, CFRP, Nanocomposite

Kaynakça

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